KMID : 0385520080210050438
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Analytical Science & Technology 2008 Volume.21 No. 5 p.438 ~ p.441
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Quantitative analysis of phosphorus by HERETIC-NMR method
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Lim Heon-Sung
Park Chan-Jo Lee Sueg-Geun
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Abstract
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We have developed an alternative to the internal chemical reference based on a calibrated reference signal which is not a real NMR line but an electronically produced signal (HERETIC) and determined the phosphorus concentration using this method. The area ratio of HERETIC and sample peaks obtained from the standard samples was used to measure the concentrations of different samples directly. The analysis of phosphorus by this method showed the excellent linear regression coefficient (R2=0.9999) for the concentration range from 20 ppm to 500 ppm with HERETIC peak as reference.
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KEYWORD
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phosphorus analysis, NMR, HERETIC
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